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Aquaazido{2,2′-[o-phenylenebis(nitrilomethylidyne)]diphenolato}manganese(III) hemihydrate (2009)

Abstract
In the title compound, [Mn(C20H14N2O2)(N3)(H2O)]·0.5H2O, the MnIII ion is chelated by the N,N′,O,O′-tetradentate Schiff base ligand and further coordinated by one azide ion and one water molecule in trans positions, resulting in a distorted fac-MnN3O3 octahedral arrangement. The O atom of the uncoordinated water molecule lies on a crystallographic twofold axis. In the crystal, O—H...O and O—H...N hydrogen bonds help to establish the packing.

Publication details
Download http://scripts.iucr.org/cgi-bin/paper?S1600536809020200
http://www.doaj.org/doaj?func=openurl&genre=article&issn=16005368&date=2009&volume=65&issue=7&spage=m707
Publisher International Union of Crystallography
Repository DOAJ-Articles (Sweden)
Language eng