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Tetra-μ-oxido-tetrakis{dioxido[3-(2-pyridyl)-1H-pyrazole]molybdenum(VI)} (2009)

Abstract
In the title compound, [Mo4O12(C8H7N3)4], the MoVI ion has a distorted octahedral coordination completed by two terminal O atoms, two μ-oxide atoms and two N atoms from one 3-(2-pyridyl)-1H-pyrazole ligand. It is noteworthy that in the tetranuclear unit (overline4 symmetry), any three MoVI atoms define a plane, and the fourth lies 1.8 (1) Å out of that plane. The degree of linearity of the oxide bridges between two Mo atoms is 175.38 (13)°. Moreover, the N—H group forms an intramolecular hydrogen bond (four per molecule).

Publication details
Download http://scripts.iucr.org/cgi-bin/paper?S1600536809031717
http://www.doaj.org/doaj?func=openurl&genre=article&issn=16005368&date=2009&volume=65&issue=9&spage=m1074
Publisher International Union of Crystallography
Repository DOAJ-Articles (Sweden)
Language eng